Promdet, P., Horkaew, J., Chantrapromma, S. Web of Science CrossRef PubMed CAS Google Scholar Web of Science CSD CrossRef IUCr Journals Google Scholar Web of Science CSD CrossRef CAS IUCr Journals Google Scholar Bruker AXS Inc., Madison, Wisconsin, USA. CrossRef CAS Web of Science Google Scholarīruker (2009). Web of Science CrossRef PubMed CAS Google Scholarīernstein, J., Davis, R. CrossRef Web of Science Google Scholarīedia, K.-K., Elçin, O., Seda, U., Fatma, K., Nathaly, S., Sevim, R.
O4 iv short contact was observed.įractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å 2) topĪllen, F. O interactions (Table 1) into a two-dimensional network paralell to the ab plane. Bond distances are of normal values (Allen et al., 1987) and are comparable with those found in related structures (Fun et al., 2011 Horkaew et al., 2011 Promdet et al., 2011). O3 hydrogen bond generates a S(5) ring motif (Bernstein et al., 1995). The methoxy group of 4-methoxyphenyl is slightly twisted with respect to its bound benzene ring, whereas the ethoxy group of 3-ethoxy-4-hydroxyphenyl is co-planar with the torsion angle C11–O3–C16–C17 = 178.5 (2)°.Īn intramolecular O4-H1O4 The mean plane through this bridge makes dihedral angles of 28.94 (15) and 26.51 (15)° with the C1–C6 and C9–C14 phenyl rings, respectively. of 0.0360 (2) Å for the five non-H atoms. The Duo has dual sources to collect data on routine, well-diffracting samples (using Mo radiation) as well as small and weak samples (Cu). For example, (5), C 13 H 10 OS, was incorrectly input as the sulfoxide, C. Data collection is performed on a Bruker Kappa APEX II Duo CCD diffractometer with Oxford CryoSystems CryoStream 700 Crystal Cooling System for low temperature capabilities. The middle bridge fragment (O1/C7/N1/N2/C8) is planar with the torsion angle N2–N1–C7–O1 = 0.8 (4)° and the r.m.s. Inputting the incorrect formula The effect of inputting the incorrect molecular formula was investi-gated, since it is necessary to input a formula at the start of the experiment, and in some cases the identity of the crystal may not be known. The molecule is slightly twisted with the dihedral angle between the two benzene rings of 6.86 (11)°. 1) exists in a trans-configuration with respect to the C8 ═N2 bond, as indicated by the torsion angle N1–N2–C8–C9 = -178.2 (2)°. The molecule of the title benzohydrazide derivative (Fig. POWDERLA BRUKER D8-Vario and MTC oven X-ray Powder. 
POWDERSA BRUKER D8-Focus Bragg-Brentano X-ray Powder Diffractometer. QUEST ECO BRUKER-AXS Duo Mo Photon III 3-thircle X-ray Diffractometer.
APEX22 BRUKER-AXS Duo Mo/Cu micro-source APEX-II CCD 3-thircle X-ray Diffractometer. The title compound was synthesized and tested for its antioxidant and antibacterial activities and found to be inactive. APEX21 BRUKER-AXS APEX-II CCD 3-thircle X-ray Diffractometer. During the course of our on-going research on benzohydrazide derivatives, which have been reported to possess various biological properties such as antibacterial and antifungal (Loncle et al., 2004), antitubercular (Bedia et al., 2006) and antiproliferative (Raj et al., 2007) activities, the synthesis and crystal structures of benzohydrazide derivatives have been reported (Fun et al., 2011 Horkaew et al., 2011 Promdet et al., 2011).
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